Question

那位化学英语高手帮忙翻译下论文，用翻译软件翻译得很不通顺 谢谢帮忙

2. Experimental
2.1 Synthesis of [Ni(oba)(2,2′-bipy)]n A mixture of H2oba (0.129g, 0.5mmol), NiCl2•6 H2O (0.119g, 0.5 mmol ), NaOH (1mmol, 0.04g) and distillated water(18 mL) was heated in a 25 mL stainless- steel reactor with a Teflon liner 160℃ for 120h, followed by slow cooling to room temperature. Green block crystals were obtained in 85% yield (based on Ni).
2.2 X-crystallography
Suitable single crystals were selected under a polarizing microscope and fixed with epoxy cement on fine glass fibers which were mounted on a Bruker Smart 1000 CCD diffractometer with a MoKα radiation (λ = 0.71073 Å) at 293(2) K. The hydrogen atoms bound to carbon were located by geometrically calculations. All non-hydrogen atoms were refined by full-matrix least-squares techniques. All calculations were performed by the SHELXTL 97 program [8]. Crystal data, intensity collection and structure refinement details are summarized in table 1. Selected interatomic distances and bond angles are given in table 2. CCDC: 794282.

Answer 1

2.实验
2.1 [Ni(oba)(2,2′-bipy)] 合成反应： 在25ml不锈钢反应装置中混入H2oba (0.129g, 0.5mmol), NiCl2•6 H2O (0.119g, 0.5 mmol ), NaOH (1mmol, 0.04g)，以及18ml蒸馏水，和一条线状的聚四氟乙烯，加热至160℃下120小时，然后慢慢冷却至室温。得到绿色结晶块，根据Ni含量，产出率为85%.

2.2 X-晶体学
选择适当的单个晶体在偏振光显微镜下，用环氧树脂胶固定到精细的玻璃纤维下，玻璃纤维镶嵌在Bruker Smart 1000CCD的衍生计上，在293(2)K时放射量为λ = 0.71073 Å MoKg。 氢原子结合在碳的位置由几何计算得出。所有的非氢原子由全矩阵的最小二乘法技术提炼而得出。所有的计算根据SHELXTL 97 进行 [8], 晶体数据，密度和，结构提炼细节，汇总在表格1中。 所选定的原子间距和粘合角度由表格2给出。 CCDC: 794282.

最好还能结合课本看，意思可能会更通顺一些。