Question

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吐纳麝香是一种麝香香料，具有强烈的麝香香气和粉香香气。吐纳麝香广泛用于香水香精、化妆品香精和皂用香精配方中。由于它突出的粉香香气，因而常用于皂用香精配方中。
根据文献报导，合成吐纳麝香主要有两步反应：首先是在三氯化铝存在下由对异丙基甲苯与六碳的烯烃或醇反应形成六甲基蔡满(HMT )，然后HMT酞化成吐纳麝香。
六甲基蔡满(HMT)是合成吐纳麝香的重要中间体。 HMT的合成一般是以三氯化铝为催化剂，由对异丙基甲苯与新己烯、或2,3一二甲基一2一丁烯等六碳烯烃反应生成。本文以对异丙烯甲苯为原料合成HMT，有效的节约了生产成本。
本文以对异丙烯甲苯为原料，创新性地进行了产品深度开发研究，得到了符合高标准质量及收率要求的对异丙烯甲苯，为上业化生产奠定了坚实的基础。
以对异丙基甲苯为原料合成对异丙烯甲苯，采用减压间歇精馏方法，实现了对异丙基甲苯和对异丙烯甲苯的分离。确定了适宜的变回流比等条件，获得了含量90%以上的单一产品。

Answer 1

Musk is a blessing of musk perfume, with a strong aroma of musk and powder Hong aroma. Widely used in the grander scheme of things musk perfume fragrance, cosmetics and fragrance soap flavor formulations. As it highlights the Hong powder aroma, which are often used to flavor soap formula. According to historical reports, synthetic musk blessing of the main two-step reaction : First, aluminum chloride in the presence of isopropyl from toluene and carbon six or alcohol olefins reaction Cai methyl-6 (HMT) , and then into the grander scheme of things phthalic HMT musk. Cai methyl-6 (HMT) is a synthetic musk blessing of the important intermediates. HMT general synthesis is aluminum chloride as a catalyst, isopropyl - toluene right with the new hexene, or 2 January 2 3 1 2 1-butene six-olefins reaction. Based on toluene - propylene synthetic materials HMT, effectively saving the cost of production. Based on toluene - propylene as raw materials, innovative products to the depth of research and development, be consistent with the high standards of quality and yield requirements of the right-propylene toluene, on the industry for the production of laying a solid foundation. To the isopropyl toluene synthesis of propylene - toluene using decompression batch distillation method Implementation of isopropyl benzene and toluene right-propylene separation. Determine the appropriate variable reflux ratio and other conditions, access to the content of more than 90% of a single product.