Question

求大神们翻译，给力啊。。。。。。。

Crystallinity and phase purity of the reference and newmaterials containing the MFI phase was studied using powder XRD (Siemens 5005). The morphology of SBA-15 materials was determined with scanning electron microscopy (SEM) using a Philips XL30 apparatus. The transmission electron microscopy (TEM) images were recorded using a Philips CM200 instrument. 27Al MAS NMR technique (Bruker 500) was used to study the aluminum environment in the samples. Nitrogen sorption isotherms of the materials obtained were determined at -196 C using a conventional volumetric technique and a NOVA 2000 sorptiometer (Quantachrome). Prior to analysis, the samples were outgassed under vacuum at 300 C for 4 h. Acidity of the samples was followed by FT IR spectroscopy, using adsorption of pyridine as a probe molecule. The samples
were evacuated at 450 C for 2 h (10-4 Torr) prior measurement.

Answer 1

Crystallinity and phase purity of the reference and newmaterials containing the MFI phase was studied using powder XRD (Siemens 5005). The morphology of SBA-15 materials was determined with scanning electron microscopy (SEM) using a Philips XL30 apparatus. The transmission electron microscopy (TEM) images were recorded using a Philips CM200 instrument. 27Al MAS NMR technique (Bruker 500) was used to study the aluminum environment in the samples. Nitrogen sorption isotherms of the materials obtained were determined at -196 C using a conventional volumetric technique and a NOVA 2000 sorptiometer (Quantachrome). Prior to analysis, the samples were outgassed under vacuum at 300 C for 4 h. Acidity of the samples was followed by FT IR spectroscopy, using adsorption of pyridine as a probe molecule. The samples
were evacuated at 450 C for 2 h (10-4 Torr) prior measurement.中文翻译：结晶度和相纯度的参考及包含MFI 定相的新材料被研究使用XRD 粉末（西门子5005) 。通过使用一个飞利浦XL30仪器来扫描电子显微镜决定了SBA-15材料形态. 传送电子显微镜图像通过使用一个飞利浦CM2000仪器被记录了下来， 人们通过27AI MAS 技术（BRUKER500) 来研究样品中的铝环境，在零下196C 情况可以决定材料的氮吸附等温线，而且这个是通过使用一个传统的容积技术和一个NOVA 2000吸附仪来完成的.在分析之前，所有样品都必须在3000C 真空下进行4小时脱气处理，样品的酸性将由FTIR 红外线光谱进行跟踪.并使用氮笨吸附当做探针分子，在测量前，所有样品必须在450C （10-4托）下进行2小时清空.
以上纯手工翻译，希望满意并采纳，谢谢！

Answer 2

我使用了微软的bing翻译，里面有些专业术语可能翻的有问题，你再想想别的办法。
翻译结果如下：
结晶度和相纯度的参考和 newmaterials 包含的多边投资框架阶段使用粉末 XRD (西门子 5005） 进行了研究。SBA-15 材料的形态确定扫描电子显微镜 (SEM) 使用飞利浦 XL30 器具。透射电子显微镜 (TEM) 图像录使用飞利浦 CM200 文书。27Al MAS 核磁共振技术 (Bruker 500） 用于研究样本中的铝环境。氮吸附等温线获得的材料是在-196 C 使用常规的容积技术和新星 2000 sorptiometer （Quantachrome） 确定的。之前的分析，样品被 outgassed 300 C 在真空下为 4 h.样品的酸度其次是 FT 红外光谱，作为一个探针分子使用的吡啶吸附。样本
在 450 C 2 h (10-4 托) 事先测量撤离了。

Answer 3

结晶度和相纯度的参考和newmaterials包含MFI阶段是使用粉末x射线衍射研究了(西门子5005)。的形态,测定材料sba 15用扫描电子显微镜(SEM)使用飞利浦XL30装置。在透射电子显微镜(TEM)图像记录使用飞利浦CM200仪器。27 al MAS NMR技术(Bruker 500)是用于研究铝环境样品的。氮吸附等温线确定材料的获得在-196 C使用常规容积技术和一个新星2000 sorptiometer(Quantachrome)。分析之前,样本可以排除在真空在300 C为4 h。酸度的样品之后,英国《金融时报》的红外光谱法,利用吸附吡啶作为探针分子。样品
被疏散450 C 2 h(10 4托)之前的测量。